One-step solution combustion synthesis of pure Ni nanopowders with enhanced coercivity: The fuel effect

التفاصيل البيبلوغرافية
العنوان: One-step solution combustion synthesis of pure Ni nanopowders with enhanced coercivity: The fuel effect
المؤلفون: Khort, Aliaksandr, Podbolotov, K., Serrano-García, R., Gun'ko, Y. K.
المصدر: Journal of Solid State Chemistry. 253:270-276
مصطلحات موضوعية: Combustion synthesis, Magnetism, Microwave, Ni nanoparticles, Amino acids, Coercive force, Cyclohexane, Fuels, Metal fuels, Metal nanoparticles, Microwaves, Nanomagnetics, Nanoparticles, Nickel, Saturation magnetization, Synthesis (chemical), Urea, Combustion pro-cess, Enhanced coercivity, Microwave assisted, Reduction processing, Solid products, Solution combustion synthesis, Unique features
الوصف: In this paper, we report a new modified one-step combustion synthesis technique for production of Ni metal nanoparticles. The main unique feature of our approach is the use of microwave assisted foam preparation. Also, the effect of different types of fuels (urea, citric acid, glycine and hexamethylenetetramine) on the combustion process and characteristics of resultant solid products were investigated. It is observed that the combination of microwave assisted foam preparation and using of hexamethylenetetramine as a fuel allows producing pure ferromagnetic Ni metal nanoparticles with enhanced coercivity (78 Oe) and high value of saturation magnetization (52 emu/g) by one-step solution combustion synthesis under normal air atmosphere without any post-reduction processing.
وصف الملف: print
URL الوصول: https://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-283185
قاعدة البيانات: SwePub
الوصف
تدمد:00224596
1095726X
DOI:10.1016/j.jssc.2017.05.043