Academic Journal

Síntese de BaTIO3 e SrTIO3 pelo método hidrotermal assistido por micro-ondas utilizando anatase como precursor de titânio

التفاصيل البيبلوغرافية
العنوان: Síntese de BaTIO3 e SrTIO3 pelo método hidrotermal assistido por micro-ondas utilizando anatase como precursor de titânio
المؤلفون: Magalhães, Renata S., Junior, Wagner D. M., Souza, Agda E., Teixeira, Silvio R., Li, Máximo S., Longo, Elson
المصدر: Química Nova. February 2017 40(2)
بيانات النشر: Sociedade Brasileira de Química, 2017.
سنة النشر: 2017
مصطلحات موضوعية: titanates, barium, strontium, mineralizer, microwave, methods
الوصف: In this work barium titanate (BT) and strontium titanate (ST) were prepared by Microwave-Assisted Hydrothermal (MAH) method, using a Ti precursor different from those shown in the literature and various concentrations (1, 3 e 6 mol L-1) of KOH mineralizer. As a titanium precursor, an anatase complex with hydrogen peroxide were used. For the precursors of barium and strontium, chlorides were used. The materials resulting from the synthesis processes were characterized in room temperature by different techniques as like: X-Ray Diffraction (XRD), micro-Raman Spectroscopy, UV-Vis, Scanning Electron Microscopy (SEM) and Photoluminescence (PL). The results show that there were differences in crystallinity, morphology, number of phases and photoluminescence depending on the concentration of the mineralizer.
نوع الوثيقة: article
وصف الملف: text/html
اللغة: Portuguese
تدمد: 0100-4042
DOI: 10.21577/0100-4042.20160181
URL الوصول: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422017000200166
Rights: info:eu-repo/semantics/openAccess
رقم الانضمام: edssci.S0100.40422017000200166
قاعدة البيانات: SciELO
الوصف
تدمد:01004042
DOI:10.21577/0100-4042.20160181