Academic Journal

Validação e estimativa da incerteza de método para análise de licopeno e β-caroteno em polpa de tomate por cromatografia líquida de alta eficiência

التفاصيل البيبلوغرافية
العنوان: Validação e estimativa da incerteza de método para análise de licopeno e β-caroteno em polpa de tomate por cromatografia líquida de alta eficiência
المؤلفون: Alves, Adriana Barreto, Silva, Marta Gomes da, Carvalho, Paulo Roberto Nogueira, Vissotto, Lizziane Cynara, Bragagnolo, Neura
المصدر: Química Nova. January 2010 33(9)
بيانات النشر: Sociedade Brasileira de Química, 2010.
سنة النشر: 2010
مصطلحات موضوعية: tomato pulp, validation, uncertainty estimation
الوصف: A method to quantify lycopene and β-carotene in freeze dried tomato pulp by high performance liquid chromatography (HLPC) was validated according to the criteria of selectivity, sensitivity, precision and accuracy, and uncertainty estimation of measurement was determined with data obtained in the validation. The validated method presented is selective in terms of analysis, and it had a good precision and accuracy. Detection limit for lycopene and β-carotene was 4.2 and 0.23 mg 100 g-1, respectively. The estimation of expanded uncertainty (K = 2) for lycopene was 104 ± 21 mg 100 g-1 and for β-carotene was 6.4 ± 1.5 mg 100 g-1.
نوع الوثيقة: article
وصف الملف: text/html
اللغة: Portuguese
تدمد: 0100-4042
DOI: 10.1590/S0100-40422010000900025
URL الوصول: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422010000900025
Rights: info:eu-repo/semantics/openAccess
رقم الانضمام: edssci.S0100.40422010000900025
قاعدة البيانات: SciELO
الوصف
تدمد:01004042
DOI:10.1590/S0100-40422010000900025