Patent
Process for the preparation of a spreadable dispersion
العنوان: | Process for the preparation of a spreadable dispersion |
---|---|
Patent Number: | 8,927,045 |
تاريخ النشر: | January 06, 2015 |
Appl. No: | 13/435943 |
Application Filed: | March 30, 2012 |
مستخلص: | Process for the preparation of a spreadable edible dispersion wherein a mixture of oil and solid structuring agent particles is subjected to stirring and an aqueous phase and/or solid phase is gradually added to the mixture until a dispersion of the desired oil content is obtained, wherein the solid structuring agent particles have a microporous structure of submicron size particles. |
Inventors: | Barendse, Sandra Petronella (Vlaardingen, NL); Floter, Eckhard (Vlaardingen, NL); Hogervorst, Wim Theodorus (Vlaardingen, NL); Van Horsen, Dirk Simon Hendriks (Vlaardingen, NL); Huizinga, Hindrik (Vlaardingen, NL); van Kempen, Gijsbert Michiel Peter (Vlaardingen, NL) |
Claim: | 1. Process for the preparation of a spreadable edible dispersion comprising subjecting a mixture of oil and solid structuring agent particles to stirring and gradually adding an aqueous phase to the mixture until an oil continuous dispersion is obtained, said dispersion being an emulsion or a suspension, or any combination thereof, wherein the solid structuring agent particles, also described as secondary particles have a microporous structure, and said particles are agglomerates of primary particles of submicron size, said primary particles are platelets having an average thickness of 0.01-0.5 μm. |
Claim: | 2. Process according to claim 1 , wherein the solid structuring agent particles are edible lipid. |
Claim: | 3. Process according to claim 2 , wherein the lipid is a fat. |
Claim: | 4. Process according to claim 1 , wherein the solid structuring agent particles were prepared using a micronisation process wherein the solid structuring agent particles were prepared by preparing a homogeneous mixture of structuring agent and liquefied gas or supercritical gas at a pressure of 5-40 MPa and expanding the mixture through an orifice, under such conditions that a spray jet was applied in which the structuring agent was solidified and micronised. |
Claim: | 5. The process according to claim 4 wherein the homogeneous mixture consists of structuring agent and liquefied gas or supercritical gas. |
Claim: | 6. The process according to claim 4 wherein the dispersion comprises an oil continuous emulsion. |
Claim: | 7. The process according to claim 4 wherein the dispersion comprises a water-in-oil emulsion spread having a fat content of 45 wt % or less. |
Claim: | 8. The process according to claim 4 wherein the homogeneous mixture consists of structuring agent, oil and liquefied gas or supercritical gas. |
Claim: | 9. Spreadable edible dispersion obtainable by a process according to claim 1 . |
Claim: | 10. The dispersion according to claim 9 which comprises an oil continuous emulsion. |
Claim: | 11. The dispersion according to claim 9 which comprises a water-in-oil emulsion spread having a fat content of 45 wt % or less. |
Claim: | 12. The process according to claim 1 wherein the dispersion comprises an oil continuous emulsion. |
Claim: | 13. The process according to claim 1 wherein the dispersion comprises a water-in-oil emulsion spread having a fat content of 45 wt % or less. |
Claim: | 14. Process for the preparation of a spreadable edible dispersion comprising subjecting a mixture of oil and solid structuring agent particles to stirring and gradually added an aqueous phase to the mixture until a dispersion is obtained, said dispersion being an emulsion, a suspension, or foam or any combination thereof, wherein the solid structuring agent particles, also described as secondary particles have a microporous structure, and said particles are agglomerates of primary particles of submicron size, said primary particles are platelets having an average thickness of 0.01-0.5 μm wherein the solid structuring agent particles were prepared by preparing a homogeneous mixture of structuring agent and 10 wt % or more liquefied gas or supercritical gas dissolved into liquid at a pressure of 5-40 MPa and expanding the mixture through an orifice, under such conditions that a spray jet was applied in which the structuring agent was solidified and micronised. |
Claim: | 15. Process according to claim 14 wherein the solid structuring agent particles comprise edible lipid. |
Claim: | 16. Process according to claim 15 wherein the lipid comprises a fat. |
Claim: | 17. Process according to claim 14 wherein the homogeneous mixture consists of structuring agent oil and liquefied or supercritical gas. |
Claim: | 18. Process according to claim 14 wherein the homogeneous mixture consists of structuring agent and liquefied or supercritical gas. |
Claim: | 19. Process according to claim 14 wherein in the spreadable edible dispersion which is prepared, crystals of solid fat form a network throughout the liquid oil resulting in a structured fat phase imparting a semi-solid, plastic, spreadable consistency. |
Current U.S. Class: | 426/602 |
Patent References Cited: | 2521219 September 1950 Holman et al. 2615160 October 1952 Baur 2815286 December 1957 Andre 3120438 February 1964 McIntire et al. 3170799 February 1965 Feuge et al. 3270040 August 1966 Bradshaw et al. 3295986 January 1967 Saslaw et al. 3338720 August 1967 Pichel 3425843 February 1969 Japikse 3528823 September 1970 Rossen 3881005 April 1975 Thakkar et al. 3892880 July 1975 Grolitsch 4160850 July 1979 Hallstrom et al. 4226894 October 1980 Gawrilow 4232052 November 1980 Nappen 4234606 November 1980 Gawrilow 4308288 December 1981 Hara et al. 4375483 March 1983 Shuford et al. 4385076 May 1983 Crosby 4391838 July 1983 Pate 4578274 March 1986 Sugisawa et al. 4591507 May 1986 Bodor et al. 4826699 May 1989 Soe 4855157 August 1989 Tashiro et al. 4889740 December 1989 Price 4917915 April 1990 Cain et al. 5130156 July 1992 Bergquist et al. 5185173 February 1993 Bethke et al. 5186866 February 1993 Ryuo et al. 5352475 October 1994 Tholl 5391382 February 1995 Chappel 5429836 July 1995 Fuisz et al. 5447735 September 1995 Miller 5516543 May 1996 Amankonah et al. 5620734 April 1997 Wesdorp et al. 5707670 January 1998 Mehansho et al. 5916608 June 1999 Lanting et al. 6020003 February 2000 Stroh et al. 6031118 February 2000 Van Amerongen et al. 6056791 May 2000 Weidner et al. 6106886 August 2000 van Amerongen et al. 6117478 September 2000 Dubberke 6129944 October 2000 Tiainen et al. 6156370 December 2000 Huizinga et al. 6190680 February 2001 Sakurada et al. 6217920 April 2001 Van Endenburg et al. 6248389 June 2001 Biller et al. 6312752 November 2001 Lansbergen et al. 6316030 November 2001 Kropf et al. 6322842 November 2001 Reddy et al. 6352737 March 2002 Dolhaine et al. 6395324 May 2002 Effey et al. 6423326 July 2002 Shapiro 6423363 July 2002 Traska et al. 6468578 October 2002 Bodor et al. 6582749 June 2003 Merrick et al. 6743450 June 2004 Romanczyk, Jr. et al. 6800317 October 2004 Wester et al. 6827964 December 2004 Wester et al. 6929816 August 2005 Wester 7601184 October 2009 Tischendorf 8025913 September 2011 van den Berg et al. 8124152 February 2012 Janssen et al. 8147895 April 2012 Barendse et al. 2002/0034577 March 2002 Vogensen 2002/0048606 April 2002 Zawistowski 2002/0076476 June 2002 Kuil et al. 2002/0132035 September 2002 Tamarkin et al. 2002/0168450 November 2002 Drudis et al. 2003/0068425 April 2003 Khare 2003/0124228 July 2003 Goto et al. 2003/0124288 July 2003 Merziger et al. 2003/0165572 September 2003 Auriou 2003/0203854 October 2003 Pischel et al. 2004/0076732 April 2004 Valix 2004/0101601 May 2004 Loh et al. 2004/0105931 June 2004 Basheer et al. 2004/0166204 August 2004 Smith et al. 2004/0197446 October 2004 Haynes et al. 2005/0069625 March 2005 Chimel et al. 2005/0123667 June 2005 Sakuma et al. 2005/0196512 September 2005 Nakhasi et al. 2006/0019021 January 2006 Plank et al. 2006/0035871 February 2006 Auweter et al. 2006/0051479 March 2006 Chiavazza et al. 2006/0115553 June 2006 Gautam et al. 2006/0280855 December 2006 Van den Berg et al. 2008/0089978 April 2008 Grigg et al. 2008/0187645 August 2008 Ekblom et al. 2008/0193628 August 2008 Garbolino et al. 2008/0226786 September 2008 Ward et al. 2253515 May 1974 10253111 May 2004 21483 January 1981 0089082 September 1983 0237120 September 1987 0294692 December 1988 393963 April 1990 572051 March 1993 0775444 May 1997 0780058 June 1997 0796567 September 1997 0744992 October 1997 897671 February 1999 0898896 March 1999 0962150 December 1999 1114674 July 2001 1180545 February 2002 1197153 April 2002 1238589 August 2002 1285584 February 2003 1419698 May 2004 1557090 July 2005 1795257 June 2007 1815752 August 2007 2016834 January 2009 2123164 November 2009 2181604 May 2010 59051742 March 1984 WO9308699 May 1993 WO9521688 August 1995 WO9614755 May 1996 WO9619115 June 1996 WO9638047 December 1996 WO9742830 November 1997 WO9847386 October 1998 WO0041491 July 2000 WO0100046 January 2001 WO0132035 May 2001 WO0143559 June 2001 WO0166560 September 2001 WO0178529 October 2001 WO0191569 December 2001 WO02100183 December 2002 WO03043430 May 2003 WO03084337 October 2003 WO03966817 November 2003 WO03103633 December 2003 WO2004093571 November 2004 WO2005014158 February 2005 WO2005071053 August 2005 WO2005074717 August 2005 WO2005074726 August 2005 WO2006066979 June 2006 WO2006079445 August 2006 WO2006087090 August 2006 WO2006087092 August 2006 WO2006087093 August 2006 WO2007022897 March 2007 WO2007024770 March 2007 WO2007039020 April 2007 WO2007039040 April 2007 WO2007096211 August 2007 WO2007096243 August 2007 WO2008125380 October 2008 WO2009068651 June 2009 WO2010060713 June 2010 WO2010069746 June 2010 WO2010069747 June 2010 WO2010069750 June 2010 WO2010069751 June 2010 WO2010069752 June 2010 WO2010069753 June 2010 WO2011160921 December 2011 |
Other References: | Anon. 1982. The American Heritage Dictionary, 2nd edition. Houghton Mifflin Co., Boston, p. 407 & 1225. cited by examiner Van Den Enden et al., Rapid Determination of Water Droplet Size Distribution by PFG-NMR, Journal of Colloid and Interface Science, 1990, vol. 140 No. 1, 105-113. cited by applicant Assignment from FeyeCon to Unilever Nederland BV dated Jul. 17, 2003 (FeyeCon incorrectly characterized as a Unilever subsidiary). cited by applicant Co-pending application Dobenesque et al., U.S. Appl. No. 13/139,584, filed Sep. 8, 2011. cited by applicant Co-pending application Dobenesque et al., U.S. Appl. No. 13/133,956, filed Jul. 8, 2011. cited by applicant Co-pending application Bezemer et al., U.S. Appl. No. 13/139,580, filed Sep. 8, 2011. cited by applicant Co-pending application Dobenesque et al., U.S. Appl. No. 13/133,952, filed Aug. 23, 2011. cited by applicant Co-pending application van den Berg et al., U.S. Appl. No. 13/224,550, filed Sep. 2, 2011. cited by applicant Co-pending application Den Adel et al., U.S. Appl. No. 13/133,954, filed Jun. 10, 2011. cited by applicant Co-pending application Dobenesque et al., U.S. Appl. No. 13/133,955, filed Jul. 8, 2011. cited by applicant Munuklu, Experimental and Analytical Facilities, Delft University of Technology, Dec. 16, 2005, pp. 41-51. cited by applicant Munuklu et al., “Supercritical Melt Micronization Using the Particles from Gas Saturated Solution Process” American Chemical Society, 2003, 23, pp. 353-369. cited by applicant Hydrogenation, Wikipedia Hydrogenation, 10 PP. cited by applicant Interesterified fat, Wikipedia Article Sources and Contributors, 4 PP. cited by applicant Strawberry Powder Flavor GA1403, Strawberryflavor.com 2005, p. 1. cited by applicant Anonymous, Particle Sizes of Milk Powders, Dairy Ingredients, 2000 vol. 2 No. 4 p. 1, 2, Dairy Products Technology Center. cited by applicant Belitz et al., Milk and Dairy Products, Food Chemistry, 1999, pp. 470-474 and 497-498 XP-002264854—Table 10.4, Springer Verlag, Berlin. cited by applicant De Graaf, Consumption of tall oil-derived phytosterols in a chocolate matrix significantly decreases plasma total and low-density lipoprotein-cholesterol levels, British Journal of Nutrition, Jun. 18, 2002 88 pp. 479-488. cited by applicant Elvers et al, Margarines and shortenings, Ullmanns Encyclopedia of Industrial Chemistry, 1990, 5th Edition, vol. A16, 156-158. cited by applicant Fereidoon Shahidi et al, Margarine processing plants and equipment, Edible Oil and Fat Product, 2005, 5, 502 and 518. cited by applicant Fischer, May 2001, Food Ingredients and Analysis Int'l, Food Ingredients and Analysis Int'l, vol. 73, No. 3, 29-31. cited by applicant Garti et al., Stabilization of Water-in-Oil Emulsions by Submicrocrystalline a-Form Fat Particles, Journal of the American Oil Chemists' Society, 1998, 75, 12, 1825-1831. cited by applicant Gerber et al., Effect of Process-Parameters on Particles Obtained by the Rapid Expansion of Supercritical Solutions, World Congress on Particle Technology, 1998, 3, pp. 1-11. cited by applicant Gunstone et al, Food uses of oils and fats, The Lipid Handbook, 2007, Third Edition, 336-341. cited by applicant Gunstone et al, 2007, Occurrence and Characterisation of Oils and Fats, The Lipid Handbook, 3rd edition, pp. 51, 55, 63, 66 and 67. cited by applicant Gunstone et al., Polymorphism and nomenclature of lipid crystal forms, The Lipid Handbook, 1995, 8.1.3, Chapman & Hall. cited by applicant Gunstone, The Lipid Handbook, The Lipid Handbook 1994, 2nd ED, 321, Chapman & Hall. cited by applicant Van Den Enden, A method for the determination of the solid phase content of fats using pulse nuclear magnetic resonance, Fette Seifen Anstrichmittel, Sep. 23, 1977, 80, 180-186. cited by applicant Kochhar, Influence of Processing on Sterols of Edible Vegetable Oils, Prog. Lipid Res., 1983 vol. 22 pp. 161-188, Pergamon Press Ltd. cited by applicant Lipson et al, Interpretation of X-ray Powder diffraction Patterns, H Lipson and H Steeple 1970, chapter 9, 244-263. cited by applicant Lopez et al, Milk fat and primary fractions obtained by dry fractionation1.Chemical composition and crystallisation properties, Chemistry and Physics of Lipids, 2006, 144, 17-33, Elsevier. cited by applicant Micallef et al., Beyond blood lipids: phytosterols, statins and omega-3 polyunsaturated fatty acid therapy for hyperlipidemia, Journal of Nutritional Biochemistry, Jun. 19, 2009, 20, 927-939, Elsevier. cited by applicant Pernetti et al., Structuring of edible oils by alternatives to crystalline fat, Colloid & Interface Science, Jul. 18, 2007, vol. 12, 221-231. cited by applicant |
Primary Examiner: | Paden, Carolyn |
Attorney, Agent or Firm: | McGowan, Jr., Gerard J. |
رقم الانضمام: | edspgr.08927045 |
قاعدة البيانات: | USPTO Patent Grants |
الوصف غير متاح. |