Academic Journal

Characterization of materials in the late 15th-century animal encyclopedia at an Ottoman Library and detection of deterioration products by HPLC–DAD

التفاصيل البيبلوغرافية
العنوان: Characterization of materials in the late 15th-century animal encyclopedia at an Ottoman Library and detection of deterioration products by HPLC–DAD
المؤلفون: Emine Torgan Güzel, Recep Karadag, Nil Baydar
المصدر: Heritage Science, Vol 11, Iss 1, Pp 1-16 (2023)
بيانات النشر: SpringerOpen, 2023.
سنة النشر: 2023
المجموعة: LCC:Fine Arts
LCC:Analytical chemistry
مصطلحات موضوعية: Islamic manuscript, Iron-gall ink, Vegatable tanning, Deterioration, Leather, HPLC–DAD, Fine Arts, Analytical chemistry, QD71-142
الوصف: Abstract There are many manuscripts in institutions that preserve and exhibit cultural heritage such as museums, galleries, and libraries. These manuscripts are of great value because of their witnessing to the past and the historical and cultural significance they have accumulated. In addition to the organic nature and the natural aging of the paper, which is generally used as the primary carrier material in these objects, other materials used in the manuscripts are an obstacle to their preservation and reaching future generations. In this study, the 62-volume animal encyclopedia, which is known to be written in the name of animals, plants, and Islamic science at the end of the fifteenth century (1487–1501) and added to an Ottoman Library, was examined analytically. A total of 40 samples consisting of paper, ink, dye, and leather samples were analyzed using high performance liquid chromatography with a diode array detector (HPLC–DAD). After all, information on material characterization and deterioration product(s) was obtained. As a result of the analysis, vanillic acid, and its derivatives due to the natural aging of the paper and chrysophanic acid and its derivatives caused by fungi, which are the result of unfavorable environmental factors, were determined. It was concluded that the ink used in the manuscripts was iron-gall ink. In addition, it was determined that madder, weld, buckthorn, redwood, rhubarb, or dock plants were used as dyestuffs in paper and leather samples. Also, it was deduced that the leather samples were tanned with the vegetable tanning method using tannins. Since tannic acids were determined in the dyestuff analysis of three paper samples with ink, elemental analysis was performed on black ink by scanning an electron microscope with energy-dispersive X-ray spectroscopy (SEM–EDX). As a result of this analysis, the element of iron has been detected and it has been confirmed that the black ink is iron-gall ink. It is inevitable that this study will guide conservation experts in restoration and conservation studies.
نوع الوثيقة: article
وصف الملف: electronic resource
اللغة: English
تدمد: 2050-7445
Relation: https://doaj.org/toc/2050-7445
DOI: 10.1186/s40494-023-00968-7
URL الوصول: https://doaj.org/article/87ed3d748b524506a55ee2f4879d2c8b
رقم الانضمام: edsdoj.87ed3d748b524506a55ee2f4879d2c8b
قاعدة البيانات: Directory of Open Access Journals
الوصف
تدمد:20507445
DOI:10.1186/s40494-023-00968-7