Academic Journal
Synthesis of Copper(II) Schiff Base Complex and Its Mixed Thin Layer with ZnO Nanoparticles
| العنوان: | Synthesis of Copper(II) Schiff Base Complex and Its Mixed Thin Layer with ZnO Nanoparticles |
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| المؤلفون: | Charles A, Sivaraj K, Krishnaraj S |
| المصدر: | Iranian Journal of Chemistry & Chemical Engineering, Vol 40, Iss 3, Pp 758-764 (2021) |
| بيانات النشر: | Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR, 2021. |
| سنة النشر: | 2021 |
| المجموعة: | LCC:Chemical engineering LCC:Chemistry |
| مصطلحات موضوعية: | thin layer, zno nanoparticles, copper complexes, afm, sem, Chemical engineering, TP155-156, Chemistry, QD1-999 |
| الوصف: | Cu(II) complex derived from Synthesis of N-((1H-pyrrol-2-yl)methylene)-4-methoxyaniline Schiff base(PMMA) was studied by UV-Vis, IR spectra, and EDAX. Zinc oxide was synthesized using a simple homogeneous precipitation method with zinc acetate as a starting material. The thin layer of the studied Cu(II) complex was deposited on ZnO/Si(111) substrates by a spin coating method and characterized with scanning electron microscopy (SEM), atomic force microscopy (AFM), and photoluminescence spectroscopy. The SEM images revealed that silicon surfaces are uniformly covered by the Cu(II) complex. AFM micrographs reveal that films are closely packed and granular in nature; the signature of agglomeration of grains is almost absent. For Cu(II) complex/ZnO/Si layer the most intensive fluorescence bands due to intra-ligand transitions were observed between 498 and 520 nm, the quenching of the emission band from ZnO at 360 nm (λex =320 nm) associated with various intrinsic or extrinsic lattice defects was noted. |
| نوع الوثيقة: | article |
| وصف الملف: | electronic resource |
| اللغة: | English |
| تدمد: | 1021-9986 |
| Relation: | http://www.ijcce.ac.ir/article_38104_619ab786515e762c8487a20af73e7276.pdf; https://doaj.org/toc/1021-9986 |
| DOI: | 10.30492/ijcce.2020.38104 |
| URL الوصول: | https://doaj.org/article/6ca3224553524ec48a2e2c7988b73973 |
| رقم الانضمام: | edsdoj.6ca3224553524ec48a2e2c7988b73973 |
| قاعدة البيانات: | Directory of Open Access Journals |
| تدمد: | 10219986 |
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| DOI: | 10.30492/ijcce.2020.38104 |