Academic Journal
Fabrication of high specific surface area TiO2 nanopowders by anodization of porous titanium
العنوان: | Fabrication of high specific surface area TiO2 nanopowders by anodization of porous titanium |
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المؤلفون: | Yue Lin, Qun Qian, Zhenhui Chen, Phan Dinh Tuan, Daolun Feng |
المصدر: | Electrochemistry Communications, Vol 136, Iss , Pp 107234- (2022) |
بيانات النشر: | Elsevier, 2022. |
سنة النشر: | 2022 |
المجموعة: | LCC:Chemistry |
مصطلحات موضوعية: | TiO2 nanopowders, Porous titanium, High specific surface area, High-frequency cyclic, Industrial electrochemistry, TP250-261, Chemistry, QD1-999 |
الوصف: | The specific surface area of TiO2 powders is an important factor affecting the performance. In this study, we present a simple and novel method to fabricate TiO2 nanopowders based on electrochemical anodization. TiO2 nanopowders with coral-like structure surface and maximum specific surface area of 280 m2/g were fabricated in an aqueous electrolyte containing 1 M Na2SO4 and 0.5 wt% NaF under applied potential of 10 V. Porous titanium as an anodic substrate enhances the reaction rate and promotes the shedding of nanotube fragments. The reaction yield of powders prepared at high-frequency 10 V is nearly 3.7 times higher than that prepared at constant potential 10 V. The specific surface area of the powder prepared at high-frequency-15 V is 61% higher than that prepared at constant potential 15 V. |
نوع الوثيقة: | article |
وصف الملف: | electronic resource |
اللغة: | English |
تدمد: | 1388-2481 16841727 |
Relation: | http://www.sciencedirect.com/science/article/pii/S1388248122000364; https://doaj.org/toc/1388-2481 |
DOI: | 10.1016/j.elecom.2022.107234 |
URL الوصول: | https://doaj.org/article/5358e1e412df43c1b8c7e16841727330 |
رقم الانضمام: | edsdoj.5358e1e412df43c1b8c7e16841727330 |
قاعدة البيانات: | Directory of Open Access Journals |
تدمد: | 13882481 16841727 |
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DOI: | 10.1016/j.elecom.2022.107234 |