التفاصيل البيبلوغرافية
| العنوان: |
Novel Synthesis of Sensitive Cu-ZnO Nanorod–Based Sensor for Hydrogen Peroxide Sensing |
| المؤلفون: |
Muhammad Arsalan, Imram Saddique, Miao Baoji, Azka Awais, Ilyas Khan, Mohamed A. Shamseldin, Sadok Mehrez |
| المصدر: |
Frontiers in Chemistry, Vol 10 (2022) |
| بيانات النشر: |
Frontiers Media S.A., 2022. |
| سنة النشر: |
2022 |
| المجموعة: |
LCC:Chemistry |
| مصطلحات موضوعية: |
hydrothermal method, Cu-ZnO nanorods, electrochemical sensor, H2O2 detection, sensing, Chemistry, QD1-999 |
| الوصف: |
We aimed to synthesize sensitive electrochemical sensors for hydrogen peroxide sensing by using zinc oxide nanorods grown on a fluorine-doped tin oxide electrode by using the facial hydrothermal method. It was essential to keep the surface morphology of the material (nanorods structure); due to its large surface area, the concerned material has enhanced detection ability toward the analyte. The work presents a non-enzymatic H2O2 sensor using vertically grown zinc oxide nanorods on the electrode (FTO) surfaces with Cu nanoparticles deposited on zinc oxide nanorods to enhance the activity. Scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), energy-dispersive X-Ray (EDX), X-ray diffraction (XRD), and electrochemical methods were used to characterize copper–zinc oxide nanorods. In addition to the high surface area, the hexagonal Cu-ZnO nanorods exhibited enhanced electrochemical features of H2O2 oxidation. Nanorods made from Cu-ZnO exhibit highly efficient sensitivity of 3415 μAmM−1cm−2 low detection limits (LODs) of 0.16 μM and extremely wide linear ranges (0.001–11 mM). In addition, copper-zinc oxide nanorods demonstrated decent reproducibility, repeatability, stability, and selectivity after being used for H2O2 sensing in water samples with an RSD value of 3.83%. Cu nanoparticles decorated on ZnO nanorods demonstrate excellent potential for the detection of hydrogen peroxide, providing a new way to prepare hydrogen peroxide detecting devices. |
| نوع الوثيقة: |
article |
| وصف الملف: |
electronic resource |
| اللغة: |
English |
| تدمد: |
2296-2646 |
| Relation: |
https://www.frontiersin.org/articles/10.3389/fchem.2022.932985/full; https://doaj.org/toc/2296-2646 |
| DOI: |
10.3389/fchem.2022.932985 |
| URL الوصول: |
https://doaj.org/article/3d7551bb321441d58f3a0c06ac5fefb1 |
| رقم الانضمام: |
edsdoj.3d7551bb321441d58f3a0c06ac5fefb1 |
| قاعدة البيانات: |
Directory of Open Access Journals |
Full Text Finder