Academic Journal

Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments

التفاصيل البيبلوغرافية
العنوان: Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments
المؤلفون: Göçmengil, Gönenç, Şişman Tükel, Fatma, Uzun, Fulya, Guillong, Marcel, id_orcid:0 000-0002-6920-3362, Yilmaz, Isak, Aysal, Namik, Hanilçi, Nurullah
المصدر: Bulletin of Mineral Research and Exploration, 168
بيانات النشر: Maden Tetkik Arama Genel Müdürlüğü
سنة النشر: 2022
المجموعة: ETH Zürich Research Collection
مصطلحات موضوعية: LA-ICP-MS, Geochemistry, ICP-OES, Whole-rock geochemistry
الوصف: ICP-OES and LA-ICP-MS instruments routinely used to assess the geochemical properties of the various natural and synthetic materials. In this contribution, the analytical routines and method development procedures of the ICP-OES and LA-ICP-MS facilities installed at the Istanbul University-Cerrahpasa Geological Engineering Department, Geochronology and Geochemistry Laboratory have been evaluated using well-known international rock standards. Sample preparation techniques, method development, experimental setup and measurement conditions for the both ICP-OES and LA-ICP-MS instruments were discussed and specific analyze results of NIST SRM 614, BCR-2, AGV-2, BCR-2G and AGV-2G were evaluated. Flux-free USGS glass standards were produced by in-house techniques and flux-bearing glasses were produced by fusion of sample with the mixture of ultra-pure lithium-tetraborate, lithium metaborate and lithiumbromide were evaluated and compared with the well-known reference values in the literature. Relative standard deviation (RSD) values for the major oxide measurements for standards given range of 0.0 wt. % to 1.5 wt. %. RSD values for the trace and rare-earth-elements values were mainly lower than 10 wt. %. The results confirm that the both flux-bearing and flux-free glasses reasonably match with the worldwide inter-laboratory values for international standards samples. The combination of these two instruments can be used to conduct geochemistry of various solid earth materials. ; ISSN:0026-4563
نوع الوثيقة: article in journal/newspaper
وصف الملف: application/application/pdf
اللغة: English
Relation: info:eu-repo/semantics/altIdentifier/wos/000865782300011; http://hdl.handle.net/20.500.11850/579637
DOI: 10.3929/ethz-b-000579637
الاتاحة: https://hdl.handle.net/20.500.11850/579637
https://doi.org/10.3929/ethz-b-000579637
Rights: info:eu-repo/semantics/openAccess ; http://creativecommons.org/licenses/by-nc-nd/4.0/ ; Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International
رقم الانضمام: edsbas.B50A6F8B
قاعدة البيانات: BASE
الوصف
DOI:10.3929/ethz-b-000579637