التفاصيل البيبلوغرافية
| العنوان: |
Sustainable alternative protocols for the multicomponent synthesis of spiro-4H-pyrans catalyzed by 4-dimethylaminopyridine |
| المؤلفون: |
Majid Mommahed Heravi (9225485), Masoumeh Zakeri (1551499), Mohamed MahmoudNasef (12004555), Ebrahim Abouzari-Lotf (3125853), Arezoo Moharami (12004558) |
| سنة النشر: |
2022 |
| المجموعة: |
Smithsonian Institution: Digital Repository |
| مصطلحات موضوعية: |
Organic Chemistry, Nuclear Chemistry, Non-metal Chemistry, Nanochemistry and Supramolecular Chemistry, Optical Properties of Materials, Natural Products Chemistry, Organic Green Chemistry, Organic Chemistry not elsewhere classified, Quantum Chemistry, Organometallic Chemistry, 4-Dimethylaminopyridine, Ball milling, Green chemistry, Microwave irradiation, Spiro-4H-pyrans, Catalysts, Irradiation, Milling (machining), Environmental friendliness |
| الوصف: |
Green approaches to the synthesis of spiro-4. H-pyrans are reported based on the one-pot and three-component condensation via a domino Knoevenagel /Michael /cyclization sequence. These approaches involve evaluation of the activity of several organocatalysts in water as a reaction media and also under solvent-free in both microwave irradiation and ball milling conditions. Extensive experiments were carried out to optimize the reaction parameters including type and amount of catalyst, reaction temperature and time. Microwave irradiation in presence of 4-dimethylaminopyridine (DMAP) was observed as the best procedure with good yields, short reaction time, environmental friendliness, and convenient operation. |
| نوع الوثيقة: |
article in journal/newspaper |
| اللغة: |
unknown |
| Relation: |
https://figshare.com/articles/journal_contribution/Sustainable_alternative_protocols_for_the_multicomponent_synthesis_of_spiro-4H-pyrans_catalyzed_by_4-dimethylaminopyridine/19074323 |
| DOI: |
10.6084/m9.figshare.19074323.v1 |
| الاتاحة: |
https://doi.org/10.6084/m9.figshare.19074323.v1 |
| Rights: |
CC BY 4.0 |
| رقم الانضمام: |
edsbas.ADB301B3 |
| قاعدة البيانات: |
BASE |