Academic Journal
Formation of octacalcium phosphate in the interaction of calcium carbonate and monocalcium phosphate monohydrate under galvanostatic conditions ; Формирование октакальцийфосфата при взаимодействии карбоната кальция и монокальцийфосфата моногидрата в гальваностатических условиях
| العنوان: | Formation of octacalcium phosphate in the interaction of calcium carbonate and monocalcium phosphate monohydrate under galvanostatic conditions ; Формирование октакальцийфосфата при взаимодействии карбоната кальция и монокальцийфосфата моногидрата в гальваностатических условиях |
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| المؤلفون: | V. K. Krut’ko, A. E. Doroshenko, O. N. Musskaya, S. M. Rabchynski, A. I. Kulak, В. К. Крутько, А. Е. Дорошенко, О. Н. Мусская, С. М. Рабчинский, А. И. Кулак |
| المساهمون: | The work was financially supported by the SPSR “Chemical processes, reagents and technologies, bioregulators and bioorganic chemistry” under assignment 2.1.04.7 for 2021–2025, Работа выполнена при финансовой поддержке ГПНИ «Химические процессы, реагенты и технологии, биорегуляторы и биооргхимия» по заданию 2.1.04.7 на 2021–2025 гг. |
| المصدر: | Proceedings of the National Academy of Sciences of Belarus, Chemical Series; Том 58, № 3 (2022); 263-272 ; Известия Национальной академии наук Беларуси. Серия химических наук; Том 58, № 3 (2022); 263-272 ; 2524-2342 ; 1561-8331 ; 10.29235/1561-8331-2022-58-3 |
| بيانات النشر: | The Republican Unitary Enterprise Publishing House "Belaruskaya Navuka" |
| سنة النشر: | 2022 |
| المجموعة: | Proceedings of the National Academy of Sciences of Belarus, Chemical Series / Известия Национальной академии наук Беларуси. Серия химических наук |
| مصطلحات موضوعية: | гидроксиапатит, calcite, dicalcium phosphate dehydrate, galvanostatic mode, tricalcium phosphate, hydroxyapatite, кальцит, дикальцийфосфат дигидрат, гальваностатический режим, трикальцийфосфат |
| الوصف: | The calcium phosphate composite octacalcium phosphate / calcite was obtained at pH 5–7 from the CaCO3/Ca(H2PO4)2 aqueous suspension in a galvanostatic mode at a current density of 20 mA/cm2 for 20 min. Drying at 80 °C without the precipitate maturation stage led to a powder formation consisting of brushite, calcite and a small amount of octacalcium phosphate. Prolonged maturation in air for 2 months led to the hydrolytic transformation of brushite into octacalcium phosphate stabilized by calcite. The use of electric current made it possible to increase the amount of octacalcium phosphate in the composite powder with the morphology of lamellar rosettes. Calcination at 800 °C of the composite powders led to the formation of α/β-tricalcium phosphate, β-calcium pyrophosphate, hydroxyapatite, and calcium oxide. ; Кальцийфосфатный композит октакальцийфосфат/кальцит получали в водной среде при pH 5–7 из суспензии CaCO3/Ca(H2PO4)2 в гальваностатическом режиме при плотности тока 20 мА/см2 в течение 20 мин. Высушивание при 80 °C без стадии созревания осадка приводило к получению порошка, состоящего из брушита, кальцита и малого количества октакальцийфосфата. Длительное созревание на воздухе (2 мес.) приводило к гидролитической трансформации брушита в октакальцийфосфат, стабилизированный кальцитом. Использование электрического тока позволило увеличить количество октакальцийфосфата в составе композитного порошка с морфологией пластинчатых розеток. Термообработка при 800 °C композитных порошков приводила к формированию α/β-трикальцийфосфата, β-пирофосфата кальция, гидроксиапатита и оксида кальция. |
| نوع الوثيقة: | article in journal/newspaper |
| وصف الملف: | application/pdf |
| اللغة: | Russian |
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| DOI: | 10.29235/1561-8331-2022-58-3-263-272 |
| الاتاحة: | https://vestichem.belnauka.by/jour/article/view/736 https://doi.org/10.29235/1561-8331-2022-58-3-263-272 |
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| رقم الانضمام: | edsbas.A5BE27EB |
| قاعدة البيانات: | BASE |
| DOI: | 10.29235/1561-8331-2022-58-3-263-272 |
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