التفاصيل البيبلوغرافية
| العنوان: |
Microwave Assisted Synthesis of Thiocarbamoylpyrazoles and Application as an Alternative Latent Fingermark Developers |
| المؤلفون: |
Rosa,Bruno N. da, Venzke,Dalila, Poletti,Taís, Lima,Nathalia P. K. de, Camacho,Jeanifer T., Mariotti,Kristiane C., Santos,Marco A. Z. dos, Pizzuti,Lucas, Carreño,Neftalí L. V., Pereira,Claudio M. P. |
| المصدر: |
Journal of the Brazilian Chemical Society v.31 n.6 2020 |
| بيانات النشر: |
Sociedade Brasileira de Química |
| سنة النشر: |
2020 |
| المجموعة: |
SciELO Brazil (Scientific Electronic Library Online) |
| مصطلحات موضوعية: |
pyrazole, dusting powder, latent fingermark, forensic chemistry |
| الوصف: |
Fingerprints are unique to each individual, contributing to human identification in forensic cases. The powder technique being widely used is considered one of the most important in latent fingermarks analysis. In this sense, the present work aimed to synthesize 1-thiocarbamoyl-4,5-dihydro-1H-pyrazoles and apply them as powder agents to develop latent fingermarks. The compounds were prepared from an effective and green synthesis via the condensation of chalcones with thiosemicarbazide in ethanol under microwave irradiation. Pyrazoles were tested and compared with a standard white powder (Sirchie®) on glass surfaces using sebaceous and natural fingermarks so that molecule 2c has been shown to be more promising providing image clarity. The derivatives of pyrazoles were promising as an alternative latent fingermark, presenting high quality images for fingermarks, proving to be a great tool for forensic sciences. |
| نوع الوثيقة: |
article in journal/newspaper |
| وصف الملف: |
text/html |
| اللغة: |
English |
| الاتاحة: |
http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532020000601327 |
| Rights: |
info:eu-repo/semantics/openAccess |
| رقم الانضمام: |
edsbas.417BA38E |
| قاعدة البيانات: |
BASE |