Bubble formation and lattice parameter changes resulting from He irradiation of defect-fluorite Gd2Zr2O7

التفاصيل البيبلوغرافية
العنوان: Bubble formation and lattice parameter changes resulting from He irradiation of defect-fluorite Gd2Zr2O7
المؤلفون: J. Wen, Jeffery A. Aguiar, Haizhou Xue, Maulik K. Patel, Yanwen Zhang, William J. Weber, Caitlin A. Taylor, Yongqiang Wang, Miguel L. Crespillo
المصدر: Acta Materialia. 115:115-122
بيانات النشر: Elsevier BV, 2016.
سنة النشر: 2016
مصطلحات موضوعية: 010302 applied physics, Materials science, Polymers and Plastics, Metals and Alloys, Pyrochlore, Analytical chemistry, chemistry.chemical_element, 02 engineering and technology, engineering.material, 021001 nanoscience & nanotechnology, 01 natural sciences, Fluence, Electronic, Optical and Magnetic Materials, Ion, Lattice constant, chemistry, 0103 physical sciences, Ceramics and Composites, engineering, Radiation damage, Irradiation, Liquid bubble, 0210 nano-technology, Helium, Nuclear chemistry
الوصف: Pyrochlores have long been considered as potential candidates for advanced ceramic waste-forms for the immobilization of radioactive waste nuclides. This work provides evidence that Gd2Zr2O7, often considered the most radiation tolerant pyrochlore, could be susceptible to radiation damage in the form of bubble nucleation at the highest He doses expected over geological time. Ion irradiations were utilized to experimentally simulate the radiation damage and He accumulation produced by alpha-decay. Samples were pre-damaged using 7 MeV Au3+ to induce the pyrochlore to defect-fluorite phase transformation, which would occur due to alpha-recoil damage within several hundred years of storage in a Gd2Zr2O7 waste form. These samples were then implanted to various He concentrations in order to study the long-term effects of He accumulation. Helium bubbles 1-3 nm in diameter were observed in TEM at a concentration of 4.6 at.% He. Some bubbles remained isolated, while others formed chains 10-30 nm in length parallel to the surface. GIXRD measurements showed lattice swelling after irradiating pristine Gd2Zr2O7 with 7 MeV Au3+ to a fluence of 2.2 x 10(15) Au/cm(2). An increase in lattice swelling was also measured after 2.2 x 10(15) Au/cm(2) + 2 x 10(15) He/cm(2) and 2.2 x 10(15) Au/cm(2) + 2 x 10(16) He/cm(2). A decrease in lattice swelling was measured after irradiation with 2.2 x 1015 Au/cm2 + 2 x 1017 He/cm2, the fluence where bubbles and bubble chains were observed in TEM. Bubble chains are thought to form in order to reduce lattice strain normal to the surface, which is produced by the Au and He irradiation damage. (C) 2016 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
تدمد: 1359-6454
DOI: 10.1016/j.actamat.2016.05.045
URL الوصول: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::ec6441f9556901d31a16e9148f83c7d6
https://doi.org/10.1016/j.actamat.2016.05.045
Rights: OPEN
رقم الانضمام: edsair.doi.dedup.....ec6441f9556901d31a16e9148f83c7d6
قاعدة البيانات: OpenAIRE
الوصف
تدمد:13596454
DOI:10.1016/j.actamat.2016.05.045