Pd-Catalyzed Enantioselective Dearomative Allylic Annulation to Access PPAPs Analogues

التفاصيل البيبلوغرافية
العنوان: Pd-Catalyzed Enantioselective Dearomative Allylic Annulation to Access PPAPs Analogues
المؤلفون: Junfeng Yang, Junliang Zhang, Qiaoyu Chen, Sanliang Li, Xiaoxiao Xie
المصدر: Organic letters. 23(20)
سنة النشر: 2021
مصطلحات موضوعية: Annulation, Allylic rearrangement, Bicyclic molecule, Molecular Structure, Chemistry, Organic Chemistry, Enantioselective synthesis, Stereoisomerism, Phloroglucinol, Biochemistry, Combinatorial chemistry, Catalysis, Biological property, Physical and Theoretical Chemistry, Palladium
الوصف: Polycyclic polyprenylated acylphloroglucinols (PPAPs) share a common bicyclo[3.3.1]alkenone core structure and attract numerous attention from synthetic organic chemists due to their fascinating biological properties and associated synthetic challenges. We present herein that Pd-phosphoramidite catalysts promote the enantioselective dearomative allylic annulation reaction between allyl desoxyhumulones and allylic dicarbonates, affording PPAPs analogues in good yields and enantioselectivities. The reaction likely proceeds through two-step dearomative allylation by Pd, and the C-allylation pathway is the dominant mechanistic model.
تدمد: 1523-7052
URL الوصول: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::d9fe85dff1e28f0da42d2ce49557cfeb
https://pubmed.ncbi.nlm.nih.gov/34570520
Rights: CLOSED
رقم الانضمام: edsair.doi.dedup.....d9fe85dff1e28f0da42d2ce49557cfeb
قاعدة البيانات: OpenAIRE