Localized production of human E-cadherin-derived first repeat in Escherichia coli

التفاصيل البيبلوغرافية
العنوان: Localized production of human E-cadherin-derived first repeat in Escherichia coli
المؤلفون: Jeffrey L. Urbauer, Teruna J. Siahaan, Irwan T. Makagiansar, Ramona J. Bieber Urbauer, Phuong Nguyen, Atsutoshi Ikesue
المصدر: Protein Expression and Purification. 26:449-454
بيانات النشر: Elsevier BV, 2002.
سنة النشر: 2002
مصطلحات موضوعية: Magnetic Resonance Spectroscopy, Lysis, Protein Conformation, Recombinant Fusion Proteins, Gene Expression, Peptide, medicine.disease_cause, law.invention, Affinity chromatography, law, Escherichia coli, medicine, Humans, chemistry.chemical_classification, Cadherin, Chemistry, Nuclear magnetic resonance spectroscopy, Periplasmic space, Cadherins, Molecular biology, Peptide Fragments, Culture Media, Biochemistry, Periplasm, Recombinant DNA, Electrophoresis, Polyacrylamide Gel, Biotechnology
الوصف: E-cadherin is a cell surface adhesion molecule that is expressed in both epithelial and endothelial tissues. In this study, an improved method for the simple production of the human E-cadherin-derived first repeat E-CAD1 was developed by exporting it into the periplasmic space of Escherichia coli . Localization of the recombinant protein into the periplasm allowed the isolation of E-CAD1 without cell lysis. The N-terminus of E-CAD1 is fused to a streptavidin-derived peptide to allow single-step purification using a Streptag affinity column. Optimal expression in LB medium produced 3.2 mg/L while expression in minimal medium containing 15 NH 4 Cl as the sole source of nitrogen produced 4.2 mg/L purified 15 N-labeled E-CAD1. Heteronuclear NMR spectroscopy confirmed that the purified E-CAD1 produced in this manner was correctly folded. The expression and purification protocol for unlabeled and isotopically labeled E-CAD1 permits rapid preparative production of this protein for mechanistic and structural studies.
تدمد: 1046-5928
DOI: 10.1016/s1046-5928(02)00553-3
URL الوصول: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::582b176f4aedf467e9531ef339f41d99
https://doi.org/10.1016/s1046-5928(02)00553-3
Rights: CLOSED
رقم الانضمام: edsair.doi.dedup.....582b176f4aedf467e9531ef339f41d99
قاعدة البيانات: OpenAIRE
الوصف
تدمد:10465928
DOI:10.1016/s1046-5928(02)00553-3