RETRACTED: Structure adhesion and corrosion resistance study of tungsten bisulfide doped with titanium deposited by DC magnetron co-sputtering

التفاصيل البيبلوغرافية
العنوان: RETRACTED: Structure adhesion and corrosion resistance study of tungsten bisulfide doped with titanium deposited by DC magnetron co-sputtering
المؤلفون: J. De La Roche, J.M. González, E. Restrepo-Parra, F. Sequeda, V. Alleh, T.W. Scharf
المصدر: Applied Surface Science. 320:538-543
بيانات النشر: Elsevier BV, 2014.
سنة النشر: 2014
مصطلحات موضوعية: Materials science, Energy-dispersive X-ray spectroscopy, General Physics and Astronomy, chemistry.chemical_element, Nanotechnology, Surfaces and Interfaces, General Chemistry, Tungsten, Condensed Matter Physics, Surfaces, Coatings and Films, Corrosion, Dielectric spectroscopy, chemistry, Sputtering, Cavity magnetron, Composite material, Thin film, Titanium
الوصف: a b s t r a c t Titanium-doped tungsten bisulfide thin films (WS2-Ti) were grown using a DC magnetron co-sputtering technique on AISI 304 stainless steel and silicon substrates. The films were produced by varying the Ti cathode power from 0 to 25 W. Using energy dispersive spectroscopy (EDS), the concentration of Ti in the WS2 was determined, and a maximum of 10% was obtained for the sample grown at 25 W. Moreover, the S/W ratio was calculated and determined to increase as a function of the Ti cathode power. According to transmission electron microscopy (TEM) results, at high titanium concentrations (greater than 6%), nanocomposite formation was observed, with nanocrystals of Ti embedded in an amorphous matrix of WS2. Using the scratch test, the coatings' adhesion was analyzed, and it was observed that as the Ti percentage was increased, the critical load (Lc) also increased. Furthermore, the failure type changed from plastic to elastic. Finally, the corrosion resistance was evaluated using the electrochemical impedance spectroscopy (EIS) technique, and it was observed that at high Ti concentrations, the corrosion resistance was improved, as Ti facilitates coating densification and generates a protective layer.
تدمد: 0169-4332
DOI: 10.1016/j.apsusc.2014.09.094
URL الوصول: https://explore.openaire.eu/search/publication?articleId=doi_________::f1ddcd0b4695a6a8c6569b46c42ff48b
https://doi.org/10.1016/j.apsusc.2014.09.094
Rights: CLOSED
رقم الانضمام: edsair.doi...........f1ddcd0b4695a6a8c6569b46c42ff48b
قاعدة البيانات: OpenAIRE
الوصف
تدمد:01694332
DOI:10.1016/j.apsusc.2014.09.094