A Pt/MnV2O6 nanocomposite for the borohydride oxidation reaction

التفاصيل البيبلوغرافية
العنوان: A Pt/MnV2O6 nanocomposite for the borohydride oxidation reaction
المؤلفون: Ana S. Dobrota, Natalia V. Skorodumova, Diogo M.F. Santos, Gulin Selda Pozan Soylu, Jadranka Milikić, Marta Martins, Igor A. Pašti, Gamze Bozkurt, Biljana Šljukić, Ayşe Bayrakçeken Yurtcan
المصدر: Journal of Energy Chemistry. 55:428-436
بيانات النشر: Elsevier BV, 2021.
سنة النشر: 2021
مصطلحات موضوعية: Materials science, Energy-dispersive X-ray spectroscopy, Energy Engineering and Power Technology, Infrared spectroscopy, chemistry.chemical_element, 02 engineering and technology, Chronoamperometry, 010402 general chemistry, 021001 nanoscience & nanotechnology, Borohydride, Electrocatalyst, 01 natural sciences, 7. Clean energy, 0104 chemical sciences, Dielectric spectroscopy, chemistry.chemical_compound, Fuel Technology, chemistry, Direct borohydride fuel cell, Electrochemistry, 0210 nano-technology, Platinum, Energy (miscellaneous), Nuclear chemistry
الوصف: Problems associated with carbon support corrosion under operating fuel cell conditions require the identification of alternative supports for platinum-based nanosized electrocatalysts. Platinum supported on manganese vanadate (Pt/MnV2O6) was prepared by microwave irradiation method and characterized using X-ray diffraction, Fourier-transform infrared spectroscopy, X-ray photoelectron spectroscopy, scanning electron microscopy with energy dispersive spectroscopy, and transmission electron microscopy. The borohydride oxidation reaction (BOR) on Pt/MnV2O6 was studied in highly alkaline media using voltammetry, chronoamperometry, and electrochemical impedance spectroscopy. BOR electrocatalytic activity of Pt/MnV2O6 was also compared with that of commercial Pt/C (46 wt% Pt) electrocatalyst. The apparent activation energy of BOR at Pt/MnV2O6 was estimated to be 32 kJ mol−1 and the order of reaction to be 0.51, indicating that borohydride hydrolysis proceeds in parallel with its oxidation. Long-term stability of Pt/MnV2O6 under BOR typical conditions was observed. A laboratory-scale direct borohydride fuel cell assembled with a Pt/MnV2O6 anode reached a specific power of 274 W g−1. Experimental results on Pt/MnV2O6 were complemented by DFT calculations, which indicated good adherence of Pt to MnV2O6, beneficial for electrocatalyst stability.
تدمد: 2095-4956
DOI: 10.1016/j.jechem.2020.07.029
URL الوصول: https://explore.openaire.eu/search/publication?articleId=doi_________::cbe709a1cb7601b04066102f91e8fd3f
https://doi.org/10.1016/j.jechem.2020.07.029
Rights: CLOSED
رقم الانضمام: edsair.doi...........cbe709a1cb7601b04066102f91e8fd3f
قاعدة البيانات: OpenAIRE
الوصف
تدمد:20954956
DOI:10.1016/j.jechem.2020.07.029