Isolation and characterization of cellulose nanoplatelets from the parenchyma cells of Agave salmiana

التفاصيل البيبلوغرافية
العنوان: Isolation and characterization of cellulose nanoplatelets from the parenchyma cells of Agave salmiana
المؤلفون: Nora A. Garcia-Gomez, Julio Silva-Mendoza, Odilia Pérez-Camacho, Carolina Rodríguez-Liñan, Selene Sepulveda-Guzman, L. Chávez-Guerrero
المصدر: Cellulose. 24:3741-3752
بيانات النشر: Springer Science and Business Media LLC, 2017.
سنة النشر: 2017
مصطلحات موضوعية: Materials science, Polymers and Plastics, biology, Agave salmiana, 02 engineering and technology, 010402 general chemistry, 021001 nanoscience & nanotechnology, biology.organism_classification, 01 natural sciences, 0104 chemical sciences, Nanocellulose, chemistry.chemical_compound, Crystallinity, chemistry, Chemical engineering, Transmission electron microscopy, Lignin, Acid hydrolysis, Hemicellulose, Cellulose, Composite material, 0210 nano-technology
الوصف: We present a novel nanostructure in the form of cellulose nanoplatelets (CNPs) with an inner array of entangled nanofibrils. The planar structure was isolated from the parenchyma cells of Agave salmiana first using basic pretreatment, then by dissolving lignin and hemicellulose using acid hydrolysis, and finally by modifying the cellulose with 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO). The crystallinity index was calculated following the purification process, and it was found that nanocellulose was 30% more crystalline than the raw material. Using transmission electron microscopy, it was found that the nanoplatelets comprise ~2–3 nm long cellulose entangled nanofibrils. In addition, via atomic force microscopy, the morphology of the nanoplatelets was confirmed; they were 90 nm thick for the acid hydrolyzed sample and 70 nm thick for the TEMPO-modified sample; their lateral size varied from a few to hundreds of micrometers, presenting large aspect ratios. Finally, CNPs were isolated and processed into thin paper with a thickness of 100 µm and transmittance of 86%, demonstrating great potential as a transparent film.
تدمد: 1572-882X
0969-0239
DOI: 10.1007/s10570-017-1376-9
URL الوصول: https://explore.openaire.eu/search/publication?articleId=doi_________::2f7d9f6ac3fcd6df967ba94bac8f6864
https://doi.org/10.1007/s10570-017-1376-9
Rights: CLOSED
رقم الانضمام: edsair.doi...........2f7d9f6ac3fcd6df967ba94bac8f6864
قاعدة البيانات: OpenAIRE
الوصف
تدمد:1572882X
09690239
DOI:10.1007/s10570-017-1376-9