Amino Steroids - 12-Oxygenated Heteroconanine Derivatives. Preparation and Properties

التفاصيل البيبلوغرافية
العنوان: Amino Steroids - 12-Oxygenated Heteroconanine Derivatives. Preparation and Properties
المؤلفون: G. Van De Woude, Monique Biesemans, L. van Hove
المصدر: Bulletin des Sociétés Chimiques Belges. 91:249-259
بيانات النشر: Wiley, 2010.
سنة النشر: 2010
مصطلحات موضوعية: chemistry.chemical_classification, Potassium hydroxide, Base (chemistry), chemistry.chemical_element, General Chemistry, Oxygen, chemistry.chemical_compound, chemistry, Boiling, Hofmann elimination, Organic chemistry, Degradation (geology), Epimer, Ethylene glycol
الوصف: Treatment of N-methyl-5α-conaninium iodides, diversely oxygenated at position 12, with a boiling solution of potassium hydroxide in ethylene glycol most often appears to be a satisfactory method to obtain the title compounds. The latter are free bases of reversed configuration at C-20 with regard to the starting compounds. The conversion is however never complete: the conanine base and an isomer of the normal Hofmann elimination product are always formed, occasionally together with minor degradation products. Comparison of the properties of heteroconan-3β-ols carrying an oxygen function at C-12 with those of the corresponding conan-3β-ols revealed differences which can be used as rules to distinguish the epimers of a pair. Deviations from the generally observed regularities seem to be dependent on the nature of the oxygen function located at C-12.
تدمد: 0037-9646
DOI: 10.1002/bscb.19820910311
URL الوصول: https://explore.openaire.eu/search/publication?articleId=doi_________::2061c5fabb844c20a5e46f5369efed8b
https://doi.org/10.1002/bscb.19820910311
Rights: CLOSED
رقم الانضمام: edsair.doi...........2061c5fabb844c20a5e46f5369efed8b
قاعدة البيانات: OpenAIRE
الوصف
تدمد:00379646
DOI:10.1002/bscb.19820910311